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Standard profiling protocols from Bruker were modified as follows: noesy with presaturation (noesygppr1d): FID size 64 k, dummy scans 4, number of scans: 128 for tissues, (cosy with presaturation (cosygpprqf): FID size 4 k, dummy scans 8, number of scans 4, spectral width 16.0125 ppm